4,4'-二甲基二苯甲酮合成路线 （共 247 条）
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); di-tert-butyl peroxide; 1,2-bis-(diphenylphosphino)ethane in benzene T=160°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Yang, Luo; Zeng, Tieqiang; Shuai, Qi; Guo, Xiangyu; Li, Chao-Jun
Chemical Communications, 2011 , vol. 47, # 7 p. 2161 - 2163
反应条件
tetra-(n-butyl)ammonium iodide; (Ph3P)2Pd(Ph)(I) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=25°C;
参考文献
Bumagin, N. A.; Kalinovskii, I. O.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 211
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 221
反应条件
(3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; palladium diacetate in tetrahydrofuran T=50°C; Suzuki reaction; 10 h;
参考文献
Mingji, Dai; Liang, Bo; Wang, Cuihua; You, Zejin; Xiang, Jing; Dong, Guangbin; Chen, Jiahua; Yang, Zhen
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1669 - 1673
反应条件
RhH(CO)(triphenylphosphine)3 in methanol T=80°C; P=15001.2 Torr; 18 h;
参考文献
Chemical Communications, , # 13 p. 1520 - 1521
反应条件
tetra-(n-butyl)ammonium iodide; tetracarbonylbis(μ-chloro)dirhodium(I) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=25°C;
参考文献
Bumagin, N. A.; Kalinovskii, I. O.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 211
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 221
反应条件
sodium hydroxide; copper(l) chloride in water; acetonitrile T=25°C; 0.166667 h;
参考文献
Narasimhamurthy, N.; Samuelson, A. G.
Tetrahedron Letters, 1986 , vol. 27, # 33 p. 3911 - 3912
反应条件
tris-(dibenzylideneacetone)dipalladium(0); copper(I) bromide dimethylsulfide complex; trifuran-2-yl-phosphane in toluene T=110°C; Carbonylative-Stille coupling; 15 h;
参考文献
Dubbaka, Srinivas Reddy; Vogel, Pierre
Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15292 - 15293
反应条件
sodium carbonate; palladium diacetate in acetone T=20°C; Suzuki reaction; 6 h;
参考文献
Korolev; Bumagin
Russian Chemical Bulletin, 2004 , vol. 53, # 2 p. 364 - 369
反应条件
silica gel supported aluminium trichloride T=80°C; Friedel Crafts acylation; 1.7 h; regioselective reaction;
参考文献
Parvanak Boroujeni, Kaveh
Turkish Journal of Chemistry, 2010 , vol. 34, # 4 p. 621 - 630
反应条件
palladium diacetate; indium in N,N-dimethyl-formamide T=20°C; P=760 Torr; 1 h;
参考文献
Zhou, Tao; Chen, Zhen-Chu
Synthetic Communications, 2002 , vol. 32, # 22 p. 3431 - 3435
