4,4'-二甲基二苯甲酮合成路线 (共 247 条)
反应条件
chlorine T=130 - 135°C;
参考文献
Connerade
Bulletin des Societes Chimiques Belges, 1933 , vol. 42, p. 311,319
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 18 h; Reflux;
参考文献
Journal of Organic Chemistry, , vol. 78, # 11 p. 5568 - 5578
反应条件
2,2'-azo-bisisobutyronitrile in tetrachloromethane T=76°C; Irradiation;
参考文献
Tetrahedron, , vol. 69, # 19 p. 3885 - 3895
反应条件
in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Hsieh, Tom H.H.; Dong, Vy M.
Tetrahedron, 2009 , vol. 65, # 16 p. 3062 - 3068
反应条件
hydrogenchloride; hydrogen sulfide in ethanol T=-5 - 10°C; 24 h;
参考文献
Ramnath, N.; Ramesh, V.; Ramamurthy, V.
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 214 - 222
反应条件
1: alcohol; hydrazine hydrate / 150 °C 2: mercury-oxide; benzene View Scheme
参考文献
Staudinger; Goldstein
Chemische Berichte, 1916 , vol. 49, p. 1924
参考文献
Ador; Crafts
Chemische Berichte, 1877 , vol. 10, p. 2175
反应条件
1: 100 percent / acetic acid / propan-2-ol / 192 h / Irradiation
2: 44 percent / iodine, acetic acid / 0.58 h / Heating
View Scheme
参考文献
Gomberg; Bachmann
Journal of the American Chemical Society, 1927 , vol. 49, p. 252
反应条件
aluminium trichloride; zinc in acetonitrile
T=35°C; 0.333333 h; irradiation of ultrasonic wave;
参考文献
Sato, Ryu; Nagaoka, Takeshi; Saito, Minoru
Tetrahedron Letters, 1990 , vol. 31, # 29 p. 4165 - 4168
反应条件
1: zinc; alcoholic NaOH-solution
2: benzene; hydrogen chloride
View Scheme
参考文献
Schneider, Reinhard; Mayr, Herbert; Plesch, Peter H.
Berichte der Bunsen-Gesellschaft, 1987 , vol. 91, p. 1369 - 1374