4,4'-二甲基二苯甲酮合成路线 （共 247 条）
反应条件
dichloro-acetic acid; oxygen in acetonitrile T=13°C; Irradiationalso in the presence of LiClO4; Product distributionRate constantMechanism;
参考文献
Gollnick, Klaus; Schnatterer, Albert; Utschick, Gerald
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 6049 - 6056
反应条件
TBANO2 in acetonitrile T=20°C; 3 h;
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 29 p. 4623 - 4626
反应条件
2,2'-bis(di-p-tolyl-phosphino)-1,1'-binaphthyl; copper(I) oxide; 1,10-phenanthroline; palladium (II) 2,4-pentanedionate in 1-methyl-pyrrolidin-2-one T=50 - 190°C; Inert atmosphereMicrowave irradiation;
参考文献
Goossen, Lukas J.; Linder, Christophe; Rodriguez, Nuria; Lange, Paul P.
Chemistry - A European Journal, 2009 , vol. 15, # 37 p. 9336 - 9349
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=60°C; 4 h;
参考文献
Rao, Maddali L. N.; Venkatesh, Varadhachari; Dasgupta, Priyabrata
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 4975 - 4980
反应条件
[2,2']bipyridinyl; sulfuric acid; water; palladium diacetate in 2-methyl-propan-1-ol T=100°C; 6 h; Inert atmosphere;
参考文献
Miao, Tao; Wang, Guan-Wu
Chemical Communications, 2011 , vol. 47, # 33 p. 9501 - 9503
反应条件
anhydrous iron chloride; potassium acetate; sodium hydrogencarbonate; iron(II) chloride T=100°C; Suzuki Coupling; P=760.051 Torr; 16 h; Schlenk technique;
参考文献
Zhong, Yanzhen; Han, Wei
Chemical Communications, 2014 , vol. 50, # 29 p. 3874 - 3877
反应条件
copper dichloride; palladium dichloride in acetic acid T=25°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 74, # 7 p. 1343 - 1348
反应条件
1: bromobenzene; oxalyl dichloride With aluminium trichloride in dichloromethane T=5 - 20°C; Friedel-Crafts reaction; 2 h; 2: toluene in dichloromethane T=20°C; 20 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 8 p. 2693 - 2702
反应条件
hydrogen fluoride; boron trifluoride T=45°C; P=37503.8 - 60006 Torr; 1 h; Further byproducts.;
参考文献
Synthesis, , # 15 p. 2543 - 2550
反应条件
[Cu(Phen)(PPh3)2]NO3; palladium diacetate in 1-methyl-pyrrolidin-2-one T=170°C; 1 h; SonicationContinuous flow reactor;
参考文献
Lange, Paul P.; Goossen, Lukas J.; Podmore, Philip; Underwood, Toby; Sciammetta, Nunzio
Chemical Communications, 2011 , vol. 47, # 12 p. 3628 - 3630
