4,4'-二甲基二苯甲酮合成路线 (共 247 条)
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); di-tert-butyl peroxide; triphenylphosphine in benzene T=150°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Chemical Communications, , vol. 47, # 7 p. 2161 - 2163
反应条件
(IPr)AuCl; oxygen in toluene T=50°C; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 33 p. 9070 - 9075
反应条件
iodine in neat (no solvent) T=85°C; 0.25 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 12 p. 1978 - 1999
反应条件
potassium hydroxide in methanol 18 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 5 p. 1371 - 1378
反应条件
BrClMg; Pd Complex; palladium in tetrahydrofuran P=22800 Torr; 16 h; Ambient temperature; Yield given;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
反应条件
Oxonereg;; 18-crown-6 ether; potassium hydrogencarbonate; acetone in water; benzene 2 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 12 p. 3043 - 3046
反应条件
manganese triacetate in acetic acid 0.05 h; Heating;
参考文献
Heterocycles, , vol. 54, # 1 p. 171 - 183
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 4 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 51, # 38 p. 4975 - 4980
反应条件
sodium hydroxide; pentacarbonyliron(0); tetrabutylammomium bromide in water; benzene T=70°C; 52 h; Further byproducts given;
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 1 p. 75 - 82
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; dichloromethane T=20°C; Cycloaddition; aromatization; desulfurization; 0.333333 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 73, # 1 p. 155 - 161