4,4'-二羟基二苯甲酮合成路线 （共 99 条）
反应条件
hydroxylamine hydrochloride; sodium acetate; toluene-2-sulfonic acid in ethanol; water; acetic acid
参考文献
The Dow Chemical Company
Patent: US5463091 A1, 1995 ;
反应条件
potassium carbonate in acetone 12 h; Heating;
参考文献
Journal of Physical Chemistry A, , vol. 109, # 12 p. 2728 - 2740
参考文献
Qi, Qingkai; Liu, Yifei; Fang, Xiaofeng; Zhang, Yumo; Chen, Peng; Wang, Yi; Yang, Bing; Xu, Bin; Tian, Wenjing; Zhang, Sean Xiao-An
RSC Advances, 2013 , vol. 3, # 21 p. 7996 - 8002
反应条件
potassium carbonate; acetone
参考文献
Nakazawa et al.
Yakugaku Zasshi, 1954 , vol. 74, p. 495
Chem.Abstr., 1955 , p. 8182
反应条件
sulfuric acid T=150°C;
参考文献
Graebe; Eichengruen
Justus Liebigs Annalen der Chemie, 1892 , vol. 269, p. 319
参考文献
Graebe; Eichengruen
Justus Liebigs Annalen der Chemie, 1892 , vol. 269, p. 319
反应条件
sulfuric acid in methanol T=50°C; 0.5 h;
参考文献
Morgan, Lee Roy; Thangaraj, Kanappan; LeBlanc, Blaise; Rodgers, Andrew; Wolford, Lionel T.; Hooper, Catherine L.; Fan, Dominic; Jursic, Branko S.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 21 p. 4552 - 4563
反应条件
sodium hydroxide in dichloromethane T=20°C; 48 h;
参考文献
Dong, Yifan; Wang, Weilun; Zhong, Cewen; Shi, Jianbing; Tong, Bin; Feng, Xiao; Zhi, Junge; Dong, Yuping
Tetrahedron Letters, 2014 , vol. 55, # 8 p. 1496 - 1500
反应条件
phosphorus trichoride Erhitzen des Reaktionsproduktes mit Phenol und etwas Schwefelsaeure auf 140grad;
参考文献
Caro; Graebe
Chemische Berichte, 1878 , vol. 11, p. 1350
反应条件
Destillieren des ueberschuessigen PCl3 ab,Erhitzen des Rueckstandes mit Phenol und konz.Schwefelsaeure;
参考文献
Caro; Graebe
Chemische Berichte, 1878 , vol. 11, p. 1350
