4,4'-二羟基二苯甲酮合成路线 （共 99 条）
参考文献
Caro; Graebe
Chemische Berichte, 1878 , vol. 11, p. 1350
反应条件
1.1: 91 percent / TiCl4; Zn / tetrahydrofuran / 2 h / Heating 2.1: Cs2CO3 / dimethylformamide / 0.17 h / 70 - 80 °C 2.2: dimethylformamide / 1.5 h / 70 - 80 °C View Scheme
参考文献
Olier-Reuchet, Chantal; Aitken, David J.; Bucourt, Robert; Husson, Henri-Philippe
Tetrahedron Letters, 1995 , vol. 36, # 45 p. 8221 - 8224
反应条件
Reaktion ueber mehrere Stufen;
参考文献
Baeyer; Burkhardt
Justus Liebigs Annalen der Chemie, 1880 , vol. 202, p. 133
反应条件
hydrogen; palladium on activated charcoal in ethanol T=20°C; 6 h;
参考文献
Hejaz, Hatem A. M.; Woo, L. W. Lawrence; Purohit, Atul; Reed, Michael J.; Potter, Barry V. L.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 10 p. 2759 - 2772
反应条件
hydrogenchloride; sodium cyanoborohydride in tetrahydrofuran 24 h; Product distribution;
参考文献
Synthetic Communications, , vol. 15, # 14 p. 1315 - 1324
反应条件
unter Druck.Hydrogenation;
参考文献
Levine; Temin
Journal of Organic Chemistry, 1957 , vol. 22, p. 85
反应条件
1.1: titanium tetrachloride; zinc / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Reflux; Darkness 2.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 70 - 80 °C 2.2: 1.75 h View Scheme
参考文献
Ding, Song; Qiao, Xin; Kucera, Gregory L.; Bierbach, Ulrich
Chemical Communications, 2013 , vol. 49, # 24 p. 2415 - 2417
反应条件
1: 40 percent / cesium carbonate / dimethylformamide / 16 h / 80 °C 2: zinc, TiCl4 / tetrahydrofuran / 5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 11 p. 3890 - 3893
参考文献
Papageorgiou, George; Corrie, John E.T.
Tetrahedron, 2005 , vol. 61, # 3 p. 609 - 616
反应条件
sodium hydride 1.) THF, mineral oil, room temperature, 30 min, 2.) THF, mineral oil, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gauthier, Sylvain; Mailhot, Josee; Labrie, Fernand
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3890 - 3893
