4-苯氨磺酰基丁烷-2-酮合成路线 （共 12 条）
反应条件
sodium perchlorate in ethanol T=25°C; Rate constant;
参考文献
Marshall,D.R. et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1977 , p. 1898 - 1909
反应条件
in acetonitrile
electrolysis (0.01-0.1 N Et4NBr or Bu4NBr, Pt cathode, Mg anode);
参考文献
Liu, Hong; Cohen, Theodore
Journal of Organic Chemistry, 1995 , vol. 60, # 7 p. 2022 - 2025
反应条件
1: diphenyldisulfane With bis(cyclopentadienyl)titanium dichloride; zinc in tetrahydrofuran
T=20°C; Inert atmosphere;
2: methyl vinyl ketone in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere;
参考文献
Xu, Xiao Bo; Yin, Xian Hong; Zhu, Yu Yang; Xu, Xin Hua; Luo, Tao; Li, Yin Hui; Lu, Xiong; Shao, Ling Ling; Pan, Jian Gao; Yang, Rong Hua
Journal of Chemical Research, 2009 , # 12 p. 750 - 752
反应条件
1: With titanium tetrachloride; magnesium in tetrahydrofuran
T=0°C; 1.05 h; Inert atmosphere;
2: With water; potassium carbonate
Inert atmosphere; chemoselective reaction;
参考文献
Lin, Kuo-Wei; Tsai, Chi-Hui; Hsieh, L-Lin; Yan, Tu-Hsin
Organic Letters, 2008 , vol. 10, # 10 p. 1927 - 1930
反应条件
air; Antifoam; Rhodococcus rhodochrous IFO 15564 in phosphate buffer
T=30°C; Oxidation; pH=6.0; 24 h;
参考文献
Ohtsuka, Yoshikazu; Katoh, Osamu; Sugai, Takeshi; Ohta, Hiromichi
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 483 - 491
反应条件
Co(eobe); phenyl silane in tetrahydrofuran
17 h; Heating;
参考文献
Friend, Christopher L.; Simpkins, Nigel S.; Anson, Michael; Polywka, Mario E. C.
Tetrahedron, 1998 , vol. 54, # 12 p. 2801 - 2808
反应条件
ethanol; benzenethiol sodium salt
参考文献
Yamagishi
Nippon Kagaku Zasshi, 1959 , vol. 80, p. 764
Chem.Abstr., 1961 , p. 3493
反应条件
sulfuric acid
1) pentane, room temperature, 6 h 2) CCl4, 60-65 deg C, 5 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kobesheva, N. I.; Kheruze, Yu. I.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1226 - 1232
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 6 p. 1381 - 1388
反应条件
(i) CCl4, (ii) aq. MeOH; Multistep reaction;
参考文献
Muraki,M. et al.
Bulletin of the Chemical Society of Japan, 1975 , vol. 48, p. 3200 - 3204
反应条件
Yield given. Multistep reaction;
参考文献
Ahlbrecht, Hubertus; Ibe, Marcellinus
Synthesis, 1988 , # 3 p. 210 - 214
