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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
61100-11-6
合成路线
（共 8 条）
40808-21-7
+
64-17-5
乙醇
→
反应条件
61100-11-6
反应条件
sulfuric acid in toluene 7 h; Heating;
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
40808-08-0
+
623-51-8
巯基乙酸乙酯
→
反应条件
61100-11-6
反应条件
1: With pyridine; triethylamine T=10 - 15°C; 1 h; 2: With potassium hydroxide 0.25 h; Cooling with ice;
参考文献
Mavrova, Anelia Ts.; Wesselinova, Diana; Tsenov, Yordan A.; Denkova, Pavletta
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 1 p. 63 - 69
16939-04-1
(4-噻吩-2-苯基)甲醇
→
反应条件
61100-11-6
反应条件
1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 2: 76 percent / NaOH; Ag2O / H2O / 20 - 50 °C 3: 95 percent / H2SO4 / toluene / 7 h / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
38401-68-2
→
反应条件
61100-11-6
反应条件
1: 76 percent / NaOH; Ag2O / H2O / 20 - 50 °C 2: 95 percent / H2SO4 / toluene / 7 h / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
108-88-3
甲苯
→
反应条件
61100-11-6
反应条件
1.1: AlCl3 / CS2 / 2.5 h / 20 °C 2.1: dimethylformamide / 22 h / 5 °C 3.1: H2SO4 / methanol / 1 h / Heating 3.2: chloranil / benzene / 2 h / Heating 4.1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 5.1: 76 percent / NaOH; Ag2O / H2O / 20 - 50 °C 6.1: 95 percent / H2SO4 / toluene / 7 h / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
38425-26-2
4-氯-4`-甲基苯丁酮
→
反应条件
61100-11-6
反应条件
1.1: dimethylformamide / 22 h / 5 °C 2.1: H2SO4 / methanol / 1 h / Heating 2.2: chloranil / benzene / 2 h / Heating 3.1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 4.1: 76 percent / NaOH; Ag2O / H2O / 20 - 50 °C 5.1: 95 percent / H2SO4 / toluene / 7 h / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
649569-55-1
→
反应条件
61100-11-6
反应条件
1.1: H2SO4 / methanol / 1 h / Heating 1.2: chloranil / benzene / 2 h / Heating 2.1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 3.1: 76 percent / NaOH; Ag2O / H2O / 20 - 50 °C 4.1: 95 percent / H2SO4 / toluene / 7 h / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
61100-11-6
→
反应条件
62403-12-7
反应条件
hydrazine hydrate in ethanol 6 h; Reflux;
参考文献
Mavrova, Anelia Ts.; Wesselinova, Diana; Tsenov, Yordan A.; Denkova, Pavletta
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 1 p. 63 - 69
