5-溴-2-(三丁基甲锡烷基)吡啶合成路线 (共 7 条)
反应条件
triphenyl phosphite; bis(acetylacetonato) palladium in anhydrous xylene T=140°C; Stille coupling; 5 h; Inert atmosphere;
参考文献
Krompiec; Ignasiak; Stanek; Filapek; Gebarowska; Penczek
Polish Journal of Chemistry, 2009 , vol. 83, # 2 p. 245 - 262
反应条件
triphenyl phosphite; bis(acetylacetonato) palladium in anhydrous xylene T=140°C; Stille coupling; 3 h; Inert atmosphere;
参考文献
Polish Journal of Chemistry, , vol. 83, # 2 p. 245 - 262
反应条件
triphenyl phosphite; bis(acetylacetonato) palladium in anhydrous xylene T=140°C; 2 h; Inert atmosphere;
参考文献
Krompiec; Ignasiak; Stanek; Filapek; Gebarowska; Penczek
Polish Journal of Chemistry, 2009 , vol. 83, # 2 p. 245 - 262
反应条件
triphenyl phosphite; bis(acetylacetonato) palladium in anhydrous xylene T=140°C; Stille coupling; 6 h; Inert atmosphere;
参考文献
Krompiec; Ignasiak; Stanek; Filapek; Gebarowska; Penczek
Polish Journal of Chemistry, 2009 , vol. 83, # 2 p. 245 - 262
反应条件
triphenyl phosphite; bis(acetylacetonato) palladium in toluene T=120°C; Stille coupling; 7 h; Inert atmosphere;
参考文献
Polish Journal of Chemistry, , vol. 83, # 2 p. 245 - 262
反应条件
triphenyl phosphite; bis(acetylacetonato) palladium in toluene T=100°C; Stille coupling; 7 h; Inert atmosphere;
参考文献
Polish Journal of Chemistry, , vol. 83, # 2 p. 245 - 262
反应条件
1: 2,5-dibromo-pyridine With n-butyllithium in toluene
T=-78°C;
2: tributyltin chloride in toluene
参考文献
Gavina, Pablo; Tatay, Sergio
Tetrahedron Letters, 2006 , vol. 47, # 20 p. 3471 - 3473