氰基甲基 2,3,4,6-O-四乙酰基-beta-D-硫代吡喃半乳糖苷合成路线 （共 5 条）
反应条件
potassium carbonate; sodium hydrogensulfite in water; acetone T=20°C; 3 h; Cooling with ice;
参考文献
KONINKLIJKE PHILIPS ELECTRONICS N.V.; Rossin, Raffaella; Laeppchen, Tilman; Van Den Bosch, Sandra Martina; Robillard, Marc Stefan; Versteegen, Ronny Mathieu
Patent: US2013/272959 A1, 2013 ;
Location in patent: Paragraph 0152 ;
反应条件
sodium disulfite; potassium carbonate in water; acetone
参考文献
Pearce, Oliver M. T.; Fisher, Kerry D.; Humphries, Julia; Seymour, Leonard W.; Smith, Alberto; Davis, Benjamin G.
Angewandte Chemie - International Edition, 2005 , vol. 44, # 7 p. 1057 - 1061
反应条件
1: 79 percent / acetone / Heating 2: 91 percent / K2CO3; sodium metabisulfite / acetone; H2O View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 7 p. 1057 - 1061
反应条件
1: HBr/AcOH / CH2Cl2 2: 79 percent / acetone / Heating 3: 91 percent / K2CO3; sodium metabisulfite / acetone; H2O View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 7 p. 1057 - 1061
反应条件
sodium methylate in methanol
T=20°C; Inert atmosphere;
参考文献
KONINKLIJKE PHILIPS ELECTRONICS N.V.; Rossin, Raffaella; Laeppchen, Tilman; Van Den Bosch, Sandra Martina; Robillard, Marc Stefan; Versteegen, Ronny Mathieu
Patent: US2013/272959 A1, 2013 ;
Location in patent: Paragraph 0148 ;
