triethylamine in dichloromethane
T=35°C; 8 h; Yields of byproduct given;
参考文献
Chaudhry, Amirah; Hargcr, Martin J. P.; Shuff, Philippa; Thompson, Alison
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 10 p. 1347 - 1352
1: 74 percent / Heating
2: 44 percent / HCl, H2O / 4.5 h / Heating
3: oxalyl chloride / CH2Cl2 / 0.5 h
4: P4S10, DMF / dioxane / 2 h / Heating
5: H2O / acetone / 28 °C
6: NEt3 / CH2Cl2 / 8 h / 35 °C
View Scheme
参考文献
Chaudhry, Amirah; Hargcr, Martin J. P.; Shuff, Philippa; Thompson, Alison
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 10 p. 1347 - 1352
1: oxalyl chloride / CH2Cl2 / 0.5 h
2: P4S10, DMF / dioxane / 2 h / Heating
3: H2O / acetone / 28 °C
4: NEt3 / CH2Cl2 / 8 h / 35 °C
View Scheme
参考文献
Chaudhry, Amirah; Hargcr, Martin J. P.; Shuff, Philippa; Thompson, Alison
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 10 p. 1347 - 1352
1: pyridine / light petroleum
2: 74 percent / Heating
3: 44 percent / HCl, H2O / 4.5 h / Heating
4: oxalyl chloride / CH2Cl2 / 0.5 h
5: P4S10, DMF / dioxane / 2 h / Heating
6: H2O / acetone / 28 °C
7: NEt3 / CH2Cl2 / 8 h / 35 °C
View Scheme
参考文献
Chaudhry, Amirah; Hargcr, Martin J. P.; Shuff, Philippa; Thompson, Alison
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 10 p. 1347 - 1352
1: P4S10, DMF / dioxane / 2 h / Heating
2: H2O / acetone / 28 °C
3: NEt3 / CH2Cl2 / 8 h / 35 °C
View Scheme
参考文献
Chaudhry, Amirah; Hargcr, Martin J. P.; Shuff, Philippa; Thompson, Alison
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 10 p. 1347 - 1352
1: 44 percent / HCl, H2O / 4.5 h / Heating
2: oxalyl chloride / CH2Cl2 / 0.5 h
3: P4S10, DMF / dioxane / 2 h / Heating
4: H2O / acetone / 28 °C
5: NEt3 / CH2Cl2 / 8 h / 35 °C
View Scheme
参考文献
Chaudhry, Amirah; Hargcr, Martin J. P.; Shuff, Philippa; Thompson, Alison
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 10 p. 1347 - 1352
