2,3-二甲基-6,7-二氢-1氢-吲哚-4(5氢)-酮合成路线 （共 4 条）
反应条件
sodium acetate; zinc in acetic acid
1 h; Heating;
参考文献
Shvedov, V. I.; Safonova, O. A.; Bulanova, T. I.; Il'ina, A. S.; Shvarts, G. Ya.; et al.
Pharmaceutical Chemistry Journal, 1980 , vol. 14, # 11 p. 794 - 798
Khimiko-Farmatsevticheskii Zhurnal, 1980 , vol. 14, # 11 p. 67 - 71
反应条件
acetic acid; zinc in water
T=0°C; 12 h; Heating;
参考文献
CHONG KUN DANG PHARMACEUTICAL CORP.; KIM, Yuntae; LEE, Changsik; YANG, Hyun-mo; CHOI, Hojin; MIN, Jaeki; KIM, Soyoung; KIM, Dal-Hyun; HA, Nina; KIM, Jung-Min; LIM, Hyojin; KO, Eunhee
Patent: WO2013/62344 A1, 2013 ;
Location in patent: Page/Page column 23; 118; 119 ;
反应条件
in 1,4-dioxane
1 h; Reflux;
参考文献
Bergman, Jan; Stensland, Birgitta
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 1 p. 1 - 10
反应条件
1: potassium tert-butylate / tetrahydrofuran / 2.25 h / |Inert atmosphere; |Reflux
2: 1,4-dioxane / 1 h / |Reflux
View Scheme
参考文献
Bergman, Jan; Stensland, Birgitta
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 1 p. 1 - 10
