3-羟基-4-硝基苯甲醇合成路线 （共 12 条）
反应条件
borane-pyridine complex; boric acid trimethyl ester; boron trifluoride diethyl etherate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride T=20°C; 3 h;
参考文献
Palakollu, Veerabhadraiah; Kanvah, Sriram
Journal of Photochemistry and Photobiology A: Chemistry, 2014 , vol. 281, p. 18 - 26
反应条件
sodium tetrahydroborate in tetrahydrofuran; methanol; diethyl ether 0 deg C, 30 min, 0 deg C to rt, 2 h;
参考文献
La Clair, James J.
Journal of the American Chemical Society, 1997 , vol. 119, # 33 p. 7676 - 7684
反应条件
sodium borohydride in ethanol
参考文献
EP581464 A1, ;
EP 0581464 A1
反应条件
hydrogenchloride in methanol; 1,2-dichloro-ethane
反应条件
sodium tetrahydroborate in diethylene glycol dimethyl ether T=60 - 70°C; 3 h; other reagent: NaBH4/AlCl3; Yield given;
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 3 p. 394 - 400
反应条件
sodium tetrahydroborate; aluminium trichloride in diethylene glycol dimethyl ether 0.5 h; Heating; Yield given;
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 3 p. 394 - 400
参考文献
Chemische Berichte, , vol. 62, p. 1182
Chemische Berichte, , vol. 66, p. 1761,1762
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane 0 deg C, 30 min, 0 deg C to rt;
参考文献
La Clair, James J.
Journal of the American Chemical Society, 1997 , vol. 119, # 33 p. 7676 - 7684
反应条件
manganese(IV) oxide in dichloromethane 20 h;
参考文献
Olszewski; Marshalla; Sabat; Sundberg
Journal of Organic Chemistry, 1994 , vol. 59, # 15 p. 4285 - 4296
反应条件
palladium in methanol; ethyl acetate
参考文献
The Procter and Gamble Company
Patent: US2005/5370 A1, 2005 ;
