9-甲基-3-硝基-9h-咔唑合成路线 （共 15 条）
反应条件
1: H2 / Pd/C / ethanol / 23 °C 2: Et3N / CH2Cl2 / 23 °C View Scheme
参考文献
Sawicki
Journal of the American Chemical Society, 1954 , vol. 76, p. 664,666
反应条件
nitric acid in acetic acid
1 h;
参考文献
Agarwal, Alka; Agarwal, Shiv K; Bhakuni, D S
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 1 p. 44 - 49
反应条件
sodium nitrate; potassium bromide in acetic acid
T=20°C; 30 h;
参考文献
Filimonov; Kulmanakova; Yusubov; Perederina; Chi, Ki-Whan; Poleshchuk
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 7 p. 917 - 923
反应条件
sodium nitrate; potassium iodide in acetic acid
T=85°C; 10 h;
参考文献
Filimonov; Kulmanakova; Yusubov; Perederina; Chi, Ki-Whan; Poleshchuk
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 7 p. 917 - 923
反应条件
ammonium cerium(IV) nitrate; silica gel in acetonitrile
T=70 - 75°C;
参考文献
Chakrabarty; Batabyal
Synthetic Communications, 1994 , vol. 24, # 1 p. 1 - 10
反应条件
1: 31 percent / conc. HNO3 / acetic acid / 60 °C
View Scheme
参考文献
Deady; Sette
Australian Journal of Chemistry, 2001 , vol. 54, # 3 p. 177 - 180
参考文献
Deady; Sette
Australian Journal of Chemistry, 2001 , vol. 54, # 3 p. 177 - 180
反应条件
ethanol; alkaline solution
参考文献
Lindemann
Chemische Berichte, 1924 , vol. 57, p. 557
Full Text Show Details
Stevens; Tucker
Journal of the Chemical Society, 1923 , vol. 123, p. 2147
反应条件
1: Hydrolysis
2: alkaline solution; acetone
View Scheme
参考文献
Stevens; Tucker
Journal of the Chemical Society, 1923 , vol. 123, p. 2147
参考文献
Stevens; Tucker
Journal of the Chemical Society, 1923 , vol. 123, p. 2147
