顺式-1,2-二羟甲基乙烯合成路线 （共 151 条）
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=23°C; 17 h;
参考文献
Fernandez-Rivas, Carolina; Mendez, Maria; Echavarren, Antonio M.
Journal of the American Chemical Society, 2000 , vol. 122, # 6 p. 1221 - 1222
反应条件
aluminum oxide T=97 - 210°C; P=760.051 Torr; Inert atmosphere;
参考文献
Kuraray Co., Ltd.
Patent: EP2133344 A1, 2009 ;
Location in patent: Page/Page column 10 ;
反应条件
aluminum oxide T=97 - 210°C; P=760.051 Torr; Inert atmosphere;
参考文献
Kuraray Co., Ltd.
Patent: EP2133344 A1, 2009 ;
Location in patent: Page/Page column 9 ;
反应条件
tetrachloromethane; triphenylphosphine in acetonitrile Mechanism;
参考文献
Barry, Carey N.; Evans, Slayton A.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3361 - 3364
反应条件
4,4'-diaminostilbene-2,2'-disulfonic acid in dichloromethane 0.5 h; Further byproducts given. Yields of byproduct given;
参考文献
Shellhamer, Dale F.; Anstine, D. Timothy; Gallego, Kelly M.; Ganesh, Brian R.; Hanson, Aaron A.; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 4 p. 861 - 866
反应条件
benzyltrichlorostannane T=88 - 90°C; 7.7 h;
参考文献
Marton, Daniele; Slaviero, Pierangelo; Tagliavini, Giuseppe
Tetrahedron, 1989 , vol. 45, # 22 p. 7099 - 7108
反应条件
methyltrioxorhenium (VII) T=170°C; 0.5 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 49 p. 12905 - 12909
Angew. Chem., , vol. 125, # 49 p. 13143 - 13147,5
反应条件
4,4'-diaminostilbene-2,2'-disulfonic acid in dichloromethane 0.5 h; Further byproducts given. Yields of byproduct given;
参考文献
Shellhamer, Dale F.; Anstine, D. Timothy; Gallego, Kelly M.; Ganesh, Brian R.; Hanson, Aaron A.; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 4 p. 861 - 866
反应条件
sodium methylate 2 h; RefluxInert atmosphere;
参考文献
ChemSusChem, , vol. 5, # 8 p. 1578 - 1586
参考文献
Reppe et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 596, p. 65
Full Text Show Details
BASF
Patent: DE855860 , 1942 ;
