顺式-1,2-二羟甲基乙烯合成路线 （共 151 条）
反应条件
toluene-4-sulfonic acid Heating;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 104, # 12 p. 679 - 682
反应条件
hydrogen bromide in dichloromethane T=0 - 20°C; 12.3333 h; Inert atmosphere; Overall yield = 57 percent; Overall yield = 42.8 g;
参考文献
Li, Xu-Wen; Ear, Alexandre; Roger, Lukas; Riache, Nassima; Deville, Alexandre; Nay, Bastien
Chemistry - A European Journal, 2013 , vol. 19, # 48 p. 16389 - 16393
反应条件
methyltrioxorhenium (VII) T=170°C; 0.5 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 49 p. 12905 - 12909
Angew. Chem., , vol. 125, # 49 p. 13143 - 13147,5
反应条件
hydrogen; montmorillonite-diphenylphosphinepalladium(II)
P=760 Torr; 30 h; Ambient temperature;
参考文献
Chickos, James S.; Uang, Jack Y.-J.; Keiderling, Tim A.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2594 - 2596
反应条件
bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in various solvent(s)
T=150°C; 4 h;
参考文献
Seddig, B.; Alm, J.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 4 p. 711 - 716
反应条件
triethylamine in diethyl ether
T=0°C; 1 h;
参考文献
Van Assema, Sander G. A.; Ehlers, Andreas W.; De Kanter, Frans J. J.; Schakel, Marius; Spek, Anthony L.; Lutz, Martin; Lammertsma, Koop
Chemistry - A European Journal, 2006 , vol. 12, # 16 p. 4333 - 4340
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Scharf, Hans-Dieter; Frauenrath, Herbert
Chemische Berichte, 1980 , vol. 113, # 4 p. 1472 - 1479
反应条件
toluene-4-sulfonic acid
distillation;
参考文献
Nieuwenhuizen, M.S.; Kieboom, A.P.G.; Bekkum, H. van
Synthesis, 1981 , # 8 p. 612 - 613
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
4 h; Ambient temperature;
参考文献
Shing, Tony K.M.; Li, Lian-Hai; Narkunan, KeSavaram
Journal of Organic Chemistry, 1997 , vol. 62, # 6 p. 1617 - 1622
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Abuzov, B. A.; Klimovitskii, E. N.; Remizov, A. B.; Timirbaev, M. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 5 p. 794 - 799
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 5 p. 1030 - 1036
