顺式-1,2-二羟甲基乙烯合成路线 （共 151 条）
反应条件
C36H81Cl3P3Ru
T=180°C; Yield given. Yields of byproduct given;
参考文献
Tsuji, Yasushi; Yokoyama, Yasuharu; Huh, Keun-Tae; Watanabe, Yoshihisa
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3456 - 3458
反应条件
acidic cation exchanger Lewatit SC 104H; orthoformic acid triethyl ester
T=50°C; 3 h;
参考文献
Scharf, Hans-Dieter; Frauenrath, Herbert
Chemische Berichte, 1980 , vol. 113, # 4 p. 1472 - 1479
反应条件
pyridine; diphosphinidenecyclobutene-coordinated palladium in toluene
T=100°C; 4.5 h;
参考文献
Murakami, Hiromi; Matsui, Yukio; Ozawa, Fumiyuki; Yoshifuji, Masaaki
Journal of Organometallic Chemistry, 2006 , vol. 691, # 14 p. 3151 - 3156
反应条件
tetrakis(triphenylphosphine) palladium(0); carbon dioxide in dichloromethane
P=22800 Torr; 44 h; Ambient temperature;
参考文献
Sakamoto, Masato; Shimizu, Isao; Yamamoto, Akio
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 4 p. 1065 - 1078
反应条件
Mucor miehei lipase; tert-butyl methyl ether
T=25°C; 5 h;
参考文献
Ciuffreda, Pierangela; Casati, Silvana; Santaniello, Enzo
Tetrahedron Letters, 2003 , vol. 44, # 18 p. 3663 - 3665
反应条件
chlorine; sodium carbonate
T=0 - 5°C;
参考文献
Reppe et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 596, p. 65
Full Text Show Details
I.G.Farbenind.
Patent: DE734025 , 1938 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Reppe,W.
Acetylene Chemistry <New York 1949>S.130
反应条件
sodium hydride in tetrahydrofuran
Heating;
参考文献
Zhao, Ligang; Lu, Xiyan; Xu, Wei
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 4059 - 4063
参考文献
Vyas, D. M.; Chiang, Y.; Doyle, T. W.
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2037 - 2039
反应条件
sodium
1) 0-4 deg C, 2) RT, 16h;
参考文献
Vyas, D. M.; Chiang, Y.; Doyle, T. W.
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2037 - 2039
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; 24 h;
参考文献
Hernandez, Ana-Isabel; Familiar, Olga; Negri, Ana; Rodriguez-Barrios, Fatima; Gago, Federico; Karlsson, Anna; Camarasa, Maria-Jose; Balzarini, Jan; Perez-Perez, Maria-Jesus
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7766 - 7773
