1-(溴甲基)-2-甲基萘合成路线 (共 7 条)
反应条件
dipotassium hydrogenphosphate; dimethyl selenoxide in 1,2-dichloro-ethane 12 h; Heating;
参考文献
Syper; Mlochowski
Synthesis, 1984 , vol. NO. 9, p. 747 - 752
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iron(II) oxalate dihydrate T=155 - 160°C; 0.166667 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 10 p. 1737 - 1740
反应条件
N-bromosuccinmide in tetrachloromethane
Heating;
参考文献
Wang, Chenguang; Mosberg, Henry I.
Tetrahedron Letters, 1995 , vol. 36, # 21 p. 3623 - 3626
反应条件
hydrogen bromide in acetic acid
bromomethylation; 4 h; Irradiation;
参考文献
Khurana, Jitender M.; Maikap, Golak C.
Journal of the Indian Chemical Society, 1999 , vol. 76, # 4 p. 216 - 217
反应条件
hydrogen bromide; acetic acid
T=60°C;
参考文献
Ziegler; Tiemann
Chemische Berichte, 1922 , vol. 55, p. 3414
参考文献
Buu-Hoi; Lecocq
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1948 , vol. 226, p. 87
反应条件
1: NaOH / ethanol
2: HCl / ethanol
View Scheme
参考文献
Mamalis,P. et al.
Journal of the Chemical Society, 1960 , p. 229 - 238