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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
612-33-9
合成路线
（共 11 条）
64-17-5
乙醇
+
612-33-9
→
反应条件
93-89-0
安息香酸乙酯
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=20°C; P=7500750 Torr; 2 h; Solvolysis;
参考文献
Romanski, Jan; Nowak, Piotr; Kosinski, Krzysztof; Jurczak, Janusz
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5287 - 5289
612-33-9
→
反应条件
15356-60-2
D-薄荷醇
+
2216-51-5
L-薄荷醇
+
58641-29-5
+
612-33-9
反应条件
Bacillus subtilis esterase in ethanol T=30°C; pH=7.2; 12 h; aq. phosphate buffer; optical yield given as percent eeenantioselective reaction;
参考文献
Zheng, Gao-Wei; Yu, Hui-Lei; Zhang, Jian-Dong; Xu, Jian-He
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 3 p. 405 - 414
612-33-9
→
反应条件
2216-51-5
L-薄荷醇
反应条件
potassium hydroxide in methanol Ambient temperature; Yield given;
参考文献
Kim, Yong Hae; Kim, Yong Il; Kim, Joong Young
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 4 p. 633 - 634
612-33-9
→
反应条件
15356-60-2
D-薄荷醇
+
2216-51-5
L-薄荷醇
反应条件
recombinant Candida rugosa lipase LIP1 in phosphate buffer T=40°C; pH=7.2; 20 h; Enzymatic reaction; Product distributionKinetics; Further Variations:Reagents;
参考文献
Vorlova, Sandra; Bornscheuer, Uwe T.; Gatfield, Ian; Hilmer, Jens-Michael; Bertram, Heinz-Juergen; Schmid, Rolf D.
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 10 p. 1152 - 1155
71-23-8
丙醇
+
612-33-9
→
反应条件
2315-68-6
苯甲酸丙酯
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=20°C; P=7500750 Torr; 2 h; Solvolysis;
参考文献
Romanski, Jan; Nowak, Piotr; Kosinski, Krzysztof; Jurczak, Janusz
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5287 - 5289
612-33-9
→
反应条件
15356-60-2
D-薄荷醇
+
2216-51-5
L-薄荷醇
+
58641-29-5
+
612-33-9
反应条件
Bacillus subtilis esterase in ethanol T=30°C; pH=7.2; 12 h; aq. phosphate buffer; optical yield given as percent eeenantioselective reaction;
参考文献
Zheng, Gao-Wei; Yu, Hui-Lei; Zhang, Jian-Dong; Xu, Jian-He
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 3 p. 405 - 414
612-33-9
→
反应条件
15356-60-2
D-薄荷醇
+
2216-51-5
L-薄荷醇
反应条件
recombinant Candida rugosa lipase LIP1 in phosphate buffer T=40°C; pH=7.2; 20 h; Enzymatic reaction; Product distributionKinetics; Further Variations:Reagents;
参考文献
Vorlova, Sandra; Bornscheuer, Uwe T.; Gatfield, Ian; Hilmer, Jens-Michael; Bertram, Heinz-Juergen; Schmid, Rolf D.
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 10 p. 1152 - 1155
612-33-9
→
反应条件
15356-60-2
D-薄荷醇
+
2216-51-5
L-薄荷醇
+
58641-29-5
+
612-33-9
反应条件
Bacillus subtilis esterase in ethanol T=30°C; pH=7.2; 12 h; aq. phosphate buffer; optical yield given as percent eeenantioselective reaction;
参考文献
Zheng, Gao-Wei; Yu, Hui-Lei; Zhang, Jian-Dong; Xu, Jian-He
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 3 p. 405 - 414
1519-39-7
(R)-(+)-甲基对甲苯亚砜
+
612-33-9
→
反应条件
52154-24-2
反应条件
(i) nBuLi, Et2NH, (ii) /BRN= 3204412/; Multistep reaction;
参考文献
Kunieda,N. et al.
Chemistry Letters, 1978 , p. 713 - 716
612-33-9
+
51651-66-2
→
反应条件
78687-13-5
+
52154-24-2
反应条件
in tetrahydrofuran; hexane T=-78°C; 2 h; ΔG(excit.), ΔS(excit.), ΔH(excit.); Thermodynamic data;
参考文献
Kunieda, Norio; Suzuki, Akira; Kinoshita, Masayoshi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 4 p. 1143 - 1150
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