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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-硝基肉桂酸
合成路线
（共 92 条）
612-41-9
2-硝基肉桂酸
→
反应条件
94594-74-8
反应条件
1: H2, 1percent aq. NaOH / Pd/C / H2O / Ambient temperature 2: 1.) NaNO2, HCl 3: 1.) SnCl2, conc. HCl; 2.) 2.5percent HCl / 1.) 15 h; 2.) reflux, 5 min 4: p.toluenesulfonic acid / benzene / Heating 5: Na / various solvent(s) / Heating 6: 70 percent / NaOH / ethanol / Heating 7: 55 percent / neat (no solvent) / Heating 8: 71 percent / sulfur / neat (no solvent) / 0.5 h / 260 °C View Scheme
参考文献
Winters; Odasso; Conti; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 215 - 218
612-41-9
2-硝基肉桂酸
→
反应条件
94594-82-8
反应条件
1: H2, 1percent aq. NaOH / Pd/C / H2O / Ambient temperature 2: 1.) NaNO2, HCl 3: 1.) SnCl2, conc. HCl; 2.) 2.5percent HCl / 1.) 15 h; 2.) reflux, 5 min 4: p.toluenesulfonic acid / benzene / Heating 5: Na / various solvent(s) / Heating 6: 98 percent / NaOH / ethanol / Heating 7: 85 percent / neat (no solvent) / Heating 8: 90 percent / H2 / Pd/C / methanol / 6 h / Ambient temperature 9: 79 percent / Na / ethanol / 11 h / Heating View Scheme
参考文献
Winters; Odasso; Conti; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 215 - 218
612-41-9
2-硝基肉桂酸
→
反应条件
530-85-8
2-硝基苯基丙炔酸
反应条件
1: bromine View Scheme
参考文献
Baeyer
Chemische Berichte, 1880 , vol. 13, p. 2258
612-41-9
2-硝基肉桂酸
→
反应条件
56983-96-1
2-苯基吡唑并(1,5-a)喹啉
反应条件
1: H2, 1percent aq. NaOH / Pd/C / H2O / Ambient temperature 2: 1.) NaNO2, HCl 3: 1.) SnCl2, conc. HCl; 2.) 2.5percent HCl / 1.) 15 h; 2.) reflux, 5 min 4: 15.5 g / p.toluenesulfonic acid / benzene / 6 h / Heating 5: Na / various solvent(s) / 1 h / Heating 6: 83 percent / NaOH / ethanol / 2.5 h / Heating 7: sulfur / neat (no solvent) / 1 h / 260 °C View Scheme
参考文献
Winters; Odasso; Conti; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 215 - 218
612-41-9
2-硝基肉桂酸
→
反应条件
579-71-5
2-硝基苯乙烯
反应条件
quinoline; copper T=185 - 195°C;
参考文献
Zessin; Steinbach; Johannsen
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 8 p. 725 - 736
612-41-9
2-硝基肉桂酸
→
反应条件
58106-56-2
反应条件
1: sulfuric acid / Reflux 2: iron; ammonium chloride / tetrahydrofuran; ethanol; water / 1 h / 85 °C View Scheme
参考文献
Ni, Lijun; Li, Ziyuan; Wu, Fan; Xu, Jinyi; Wu, Xiaoming; Kong, Lingyi; Yao, Hequan
Tetrahedron Letters, 2012 , vol. 53, # 10 p. 1271 - 1274
612-41-9
2-硝基肉桂酸
→
反应条件
60230-69-5
反应条件
1: H2, 1percent aq. NaOH / Pd/C / H2O / Ambient temperature 2: 1.) NaNO2, HCl 3: 1.) SnCl2, conc. HCl; 2.) 2.5percent HCl / 1.) 15 h; 2.) reflux, 5 min 4: 15.5 g / p.toluenesulfonic acid / benzene / 6 h / Heating 5: Na / various solvent(s) / 1 h / Heating 6: 83 percent / NaOH / ethanol / 2.5 h / Heating 7: 80 percent / neat (no solvent) / 0.33 h / 250 °C View Scheme
参考文献
Winters; Odasso; Conti; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 215 - 218
612-41-9
2-硝基肉桂酸
→
反应条件
60230-70-8
反应条件
1: H2, 1percent aq. NaOH / Pd/C / H2O / Ambient temperature 2: 1.) NaNO2, HCl 3: 1.) SnCl2, conc. HCl; 2.) 2.5percent HCl / 1.) 15 h; 2.) reflux, 5 min 4: p.toluenesulfonic acid / benzene / Heating 5: Na / various solvent(s) / Heating 6: 70 percent / NaOH / ethanol / Heating 7: 55 percent / neat (no solvent) / Heating View Scheme
参考文献
Winters; Odasso; Conti; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 215 - 218
612-41-9
2-硝基肉桂酸
→
反应条件
60230-71-9
反应条件
1: H2, 1percent aq. NaOH / Pd/C / H2O / Ambient temperature 2: 1.) NaNO2, HCl 3: 1.) SnCl2, conc. HCl; 2.) 2.5percent HCl / 1.) 15 h; 2.) reflux, 5 min 4: p.toluenesulfonic acid / benzene / Heating 5: Na / various solvent(s) / Heating 6: 98 percent / NaOH / ethanol / Heating 7: 85 percent / neat (no solvent) / Heating View Scheme
参考文献
Winters; Odasso; Conti; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 215 - 218
612-41-9
2-硝基肉桂酸
→
反应条件
60230-74-2
反应条件
1: H2, 1percent aq. NaOH / Pd/C / H2O / Ambient temperature 2: 1.) NaNO2, HCl 3: 1.) SnCl2, conc. HCl; 2.) 2.5percent HCl / 1.) 15 h; 2.) reflux, 5 min 4: p.toluenesulfonic acid / benzene / Heating 5: Na / various solvent(s) / Heating 6: 98 percent / NaOH / ethanol / Heating 7: 85 percent / neat (no solvent) / Heating 8: 90 percent / H2 / Pd/C / methanol / 6 h / Ambient temperature View Scheme
参考文献
Winters; Odasso; Conti; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 215 - 218
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