6-溴-1,3-苯并二氧戊环-5-甲腈合成路线 (共 4 条)
反应条件
hydroxylamine hydrochloride; sodium acetate; acetic acid T=125°C; 12 h;
参考文献
MYRIAD GENETICS, INC.
Patent: WO2009/65035 A1, 2009 ;
Location in patent: Page/Page column 67 ;
反应条件
[{RuCl2(p-cymene)}2]; diphenyl acetylene in isopropyl alcohol T=100°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Chinnagolla, Ravi Kiran; Pimparkar, Sandeep; Jeganmohan, Masilamani
Chemical Communications, 2013 , vol. 49, # 30 p. 3146 - 3148
反应条件
[{RuCl2(p-cymene)}2]; diphenyl acetylene in isopropyl alcohol T=100°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Chemical Communications, , vol. 49, # 30 p. 3146 - 3148
反应条件
bromine; acetic acid
参考文献
Gazzetta Chimica Italiana, , vol. 25 II, p. 205