S-(+)-Alpha-3-(1-萘氧基)-1,2-环氧丙烷合成路线 （共 33 条）
反应条件
in isopropyl alcohol 30 h; Heating;
参考文献
Kothakonda, Kiran Kumar; Bose, D. Subhas
Chemistry Letters, 2004 , vol. 33, # 9 p. 1212 - 1213
Title/Abstract Full Text View citing articles Show Details
Subhas Bose; Narsimha Reddy; Chavhan, Sanjay W.
Synthesis, 2005 , # 14 art. no. Z03505SS, p. 2345 - 2348
参考文献
Rama Rao; Gurjar; Joshi
Tetrahedron Asymmetry, 1990 , vol. 1, # 10 p. 697 - 698
反应条件
sodium hydride in N,N-dimethyl-formamide
T=20°C;
参考文献
Fagerstroem, Alexandra; Nilsson, Mikael; Berg, Ulf; Isaksson, Roland
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 16 p. 3067 - 3076
反应条件
water in tetrahydrofuran
T=0 - 20°C; 60 h; Resolution of racemate;
参考文献
Zhu, Chengfeng; Yuan, Guozan; Chen, Xu; Yang, Zhiwei; Cui, Yong
Journal of the American Chemical Society, 2012 , vol. 134, # 19 p. 8058 - 8061
反应条件
1: With triphenylphosphine in 1,4-dioxane
T=70°C; Mitsunobu reaction; 0.166667 h;
2: With di-isopropyl azodicarboxylate in 1,4-dioxane
T=70°C; Mitsunobu reaction;
参考文献
Panchgalle, Sharad P.; Gore, Rohitkumar G.; Chavan, Subhash P.; Kalkote, Uttam R.
Tetrahedron Asymmetry, 2009 , vol. 20, # 15 p. 1767 - 1770
反应条件
Jacobsen's (R,R)-(salen)Co(III) catalyst; air; acetic acid in tetrahydrofuran
T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
Jacobsen's (S,S)-(salen)Co(III) catalyst; air; acetic acid in tetrahydrofuran
T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
C72H102Co2F12N4O12P2; water in tetrahydrofuran
T=0 - 20°C; 18 h; optical yield given as percent ee;
参考文献
Sadhukhan, Arghya; Khan, Noor-Ul H.; Roy, Tamal; Kureshy, Rukhsana I.; Abdi, Sayed H. R.; Bajaj, Hari C.
Chemistry - A European Journal, 2012 , vol. 18, # 17 p. 5256 - 5260
反应条件
1: α-naphthol With sodium hydride in N,N-dimethyl-formamide
T=20°C; 1 h;
2: (2S)-glycidyl 4-toluenesulfonate in N,N-dimethyl-formamide
4 h; Further stages.;
参考文献
Smith, Christopher B.; Buntine, Mark A.; Lincoln, Stephen F.; Wainwright, Kevin P.
Dalton Transactions, 2003 , # 15 p. 3028 - 3033
