3-(4-硝基苯基)-2-丙炔-1-醇合成路线 （共 20 条）
反应条件
manganese(IV) oxide; potassium hydroxide in benzene 0.166667 h; Ambient temperature;
参考文献
Synthesis, , vol. NO. 9, p. 728 - 729
反应条件
1: H2 / Pd/CaCO3 2: titanium isopropoxide (TIP), (+)-diethyl tartrate ((+)-DET), tert-butyl hydroperoxide (TBHP) / 168 h / -20 °C 3: NaN3/silica gel / dimethylformamide / 80 °C 4: H2O, PPh3 / tetrahydrofuran View Scheme
参考文献
Rao; Bhanu
Journal of the Chemical Society - Series Chemical Communications, 1992 , # 11 p. 859 - 860
反应条件
1: H2 / Pd/CaCO3 2: titanium isopropoxide (TIP), (+)-diethyl tartrate ((+)-DET), tert-butyl hydroperoxide (TBHP) / 168 h / -20 °C 3: NaN3/silica gel / dimethylformamide / 80 °C 4: H2O, PPh3 / tetrahydrofuran View Scheme
参考文献
Rao; Bhanu
Journal of the Chemical Society - Series Chemical Communications, 1992 , # 11 p. 859 - 860
反应条件
1: H2 / Pd/CaCO3 2: titanium isopropoxide (TIP), (+)-diethyl tartrate ((+)-DET), tert-butyl hydroperoxide (TBHP) / 168 h / -20 °C 3: NaN3/silica gel / dimethylformamide / 80 °C 4: H2O, PPh3 / tetrahydrofuran View Scheme
参考文献
Rao; Bhanu
Journal of the Chemical Society - Series Chemical Communications, 1992 , # 11 p. 859 - 860
反应条件
1: H2 / Pd/CaCO3 2: titanium isopropoxide (TIP), (+)-diethyl tartrate ((+)-DET), tert-butyl hydroperoxide (TBHP) / 168 h / -20 °C 3: NaN3/silica gel / dimethylformamide / 80 °C 4: H2O, PPh3 / tetrahydrofuran View Scheme
参考文献
Rao; Bhanu
Journal of the Chemical Society - Series Chemical Communications, 1992 , # 11 p. 859 - 860
反应条件
hydrogen; Lindlar's catalyst
参考文献
Rao; Bhanu
Journal of the Chemical Society - Series Chemical Communications, 1992 , # 11 p. 859 - 860
反应条件
copper(l) iodide; (Ph3P)2Pd(Ph)(I); triethylamine in chloroform
T=20°C; 1.25 h;
参考文献
Bumagin, N. A.; Ponomarev, A. B.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 7 p. 1433 - 1438
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 7 p. 1561 - 1566
反应条件
copper(l) iodide; triethylamine; triphenylphosphine
T=90°C; Sonogashira coupling; 24 h; Inert atmosphere;
参考文献
Lin, Bo-Nan; Huang, Shao-Hsien; Wu, Wei-Yi; Mou, Chung-Yuan; Tsai, Fu-Yu
Molecules, 2010 , vol. 15, # 12 p. 9157 - 9173
反应条件
potassium carbonate; palladium diacetate in N,N-dimethyl-formamide
T=90°C; 0.166667 h; microwave irradiation;
参考文献
Togninelli, Andrea; Gevariya, Harsukh; Alongi, Maddalena; Botta, Maurizio
Tetrahedron Letters, 2007 , vol. 48, # 28 p. 4801 - 4803
反应条件
tetrabutyl ammonium fluoride; copper diacetate
T=130 - 135°C; Sonogashira cross-coupling reaction; 14 h;
参考文献
Deng, Chen-Liang; Xie, Ye-Xiang; Yin, Du-Lin; Li, Jin-Heng
Synthesis, 2006 , # 20 p. 3370 - 3376
