2-(4-溴苯基)-1H-吲哚合成路线 （共 27 条）
反应条件
1: With palladium diacetate; dimethyl sulfoxide; trifluoroacetic acid
T=90°C; 24 h;
2: With iron
T=90°C; 2 h;
参考文献
Jadhav, Jagannath; Gaikwad, Vipul; Kurane, Rajanikant; Salunkhe, Rajashri; Rashinkar, Gajanan
Synlett, 2012 , vol. 23, # 17 p. 2511 - 2515,5
Title/Abstract Full Text Show Details
Jadhav, Jagannath; Gaikwad, Vipul; Kurane, Rajanikant; Salunkhe, Rajashri; Rashinkar, Gajanan
Synlett, 2012 , vol. 23, # 17 p. 2511 - 2515
反应条件
zinc(II) chloride
T=170°C;
参考文献
Kaji; Nagashima
Yakugaku Zasshi, 1952 , vol. 72, p. 1589
Chem.Abstr., 1953 , p. 9317
反应条件
zinc(II) chloride
T=130 - 200°C;
参考文献
Cardillo, Barbara; Giorgini, Elisabetta; Greci, Lucedio; Tosi, Giorgio; Rizzoli, Corrado; et al.
Journal of Chemical Research, Miniprint, 1992 , # 7 p. 1801 - 1830
反应条件
1: carbon disulfide; bromine
View Scheme
参考文献
Collet
Bulletin de la Societe Chimique de France, 1899 , vol. <3> 21, p. 67
反应条件
sodium hydroxide in dimethyl sulfoxide
T=20 - 25°C; 0.5 h; Yield given;
参考文献
Wojciechowski, Krzysztof; Makosa, Mieczyslaw
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 8 p. 671 - 674
反应条件
hydrogenchloride; palladium dichloride in water; acetonitrile
5 h; Inert atmosphereReflux;
参考文献
Sakai, Hayato; Tsutsumi, Ken; Morimoto, Tsumoru; Kakiuchia, Kiyomi
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 16 p. 2498 - 2502
反应条件
1: sodium sulfite / water / 5 h / 70 - 80 °C
2: palladium dichloride; silver(I) acetate; sulfuric acid / N,N-dimethyl-formamide; acetonitrile / 0.67 h / 100 °C / |Sealed tube; |Microwave irradiation
View Scheme
参考文献
Miao, Tao; Li, Pinhua; Wang, Guan-Wu; Wang, Lei
Chemistry - An Asian Journal, 2013 , vol. 8, # 12 p. 3185 - 3190
反应条件
in various solvent(s)
4 h; Heating;
参考文献
Gupta, K. C.; Manglum, P.
Journal of the Indian Chemical Society, 1988 , vol. 65, p. 223 - 225
反应条件
1: p-toluenesulfonic acid / benzene / 0.5 h / Heating
2: NaOH / dimethylsulfoxide / 0.5 h / 20 - 25 °C
View Scheme
参考文献
Wojciechowski, Krzysztof; Makosa, Mieczyslaw
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 8 p. 671 - 674
反应条件
1: p-toluenesulfonic acid / benzene / 0.5 h / Heating
2: NaOH / dimethylsulfoxide / 0.5 h / 20 - 25 °C
View Scheme
参考文献
Wojciechowski, Krzysztof; Makosa, Mieczyslaw
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 8 p. 671 - 674
