(S)-[1-[[(叔丁基)氨基]羰基]-2-甲基丙基]氨基甲酸苄酯合成路线 （共 6 条）
反应条件
(i) ClCO2Me, Et3N, CHCl3, (ii) /BRN= 605267/; Multistep reaction;
参考文献
Ugi,I.; Offermann,K.
Chemische Berichte, 1964 , vol. 97, p. 2996 - 3007
反应条件
in 1,4-dioxane
20 h;
参考文献
Zabokritskii, M. P.; Rudenko, B. A.; Chizhkov, V. P.; Mitsner, B. I.; Zvonkova, E. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 5 p. 806 - 812
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 5 p. 1045 - 1051
反应条件
1: 58.5 percent / dicyclohexylcarbodiimide / dioxane; CH2Cl2 / 1.) 0 deg C, 3 h, 2.) 20 deg C, 24 h
2: 75 percent / dioxane / 20 h
View Scheme
参考文献
Zabokritskii, M. P.; Rudenko, B. A.; Chizhkov, V. P.; Mitsner, B. I.; Zvonkova, E. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 5 p. 806 - 812
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 5 p. 1045 - 1051
反应条件
hydrogen; palladium on activated charcoal in methanol
5 h; Ambient temperature;
参考文献
Nitta, Hideaki; Yu, Donghai; Kudo, Masanobu; Mori, Atsunori; Inoue, Shohei
Journal of the American Chemical Society, 1992 , vol. 114, # 21 p. 7969 - 7975
反应条件
hydrogenchloride; hydrogen; palladium in methanol
3 h;
参考文献
Zabokritskii, M. P.; Rudenko, B. A.; Chizhkov, V. P.; Mitsner, B. I.; Zvonkova, E. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 5 p. 806 - 812
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 5 p. 1045 - 1051
反应条件
hydrogen; palladium on activated charcoal in methanol
5 h; Ambient temperature;
参考文献
Nitta, Hideaki; Yu, Donghai; Kudo, Masanobu; Mori, Atsunori; Inoue, Shohei
Journal of the American Chemical Society, 1992 , vol. 114, # 21 p. 7969 - 7975
