反应条件
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere
1.2: 0.83 h / 0 °C / Inert atmosphere
1.3: 20 °C / Inert atmosphere
2.1: AlCl3, aluminium chloride; sodium chloride / 0.03 h / 140 - 180 °C / Inert atmosphere; Reaction in melt
2.2: 1 h / 50 °C / Cooling with ice
View Scheme
参考文献
Kuttruff, Christian A.; Zipse, Hendrik; Trauner, Dirk
Angewandte Chemie - International Edition, 2011 , vol. 50, # 6 p. 1402 - 1405
