(9ci)-2,3-二氢-1-亚甲基-1H-茚-4-醇合成路线 （共 2 条）
反应条件
1: triphenyl-methyl-phosphonium iodide With potassium tert-butylate in diethyl ether
0.25 h;
2: 4-(tert-butyldimethylsilyl)oxy-1-indanone in diethyl ether
T=20°C;
3: With tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 0.5 h;
参考文献
AMOREPACIFIC CORPORATION; WOO, Byoung Young; KIM, Sun-Young; KIM, Yeonjoon; SHIN, Song Seok; KIM, Jin Kwan; LEE, Ki-Wha; KIM, Dong Hyun; LIM, Kyung Min; MOH, Joo-Hyun; JEONG, Yeon Su; CHOI, Jin Kyu; KOH, Hyun Ju; LEE, Jeongho; KIM, Hyuk; YOON, Jeong Hoon; LI, Funan; KIM, Jee-Suk; SUH, Young-Ger
Patent: WO2010/2209 A2, 2010 ;
Location in patent: Page/Page column 65 ;
WO 2010/002209 A2
反应条件
hydrogen; palladium 10 on activated carbon in methanol
P=2585.81 Torr; 1 h;
参考文献
AMOREPACIFIC CORPORATION; WOO, Byoung Young; KIM, Sun-Young; KIM, Yeonjoon; SHIN, Song Seok; KIM, Jin Kwan; LEE, Ki-Wha; KIM, Dong Hyun; LIM, Kyung Min; MOH, Joo-Hyun; JEONG, Yeon Su; CHOI, Jin Kyu; KOH, Hyun Ju; LEE, Jeongho; KIM, Hyuk; YOON, Jeong Hoon; LI, Funan; KIM, Jee-Suk; SUH, Young-Ger
Patent: WO2010/2209 A2, 2010 ;
Location in patent: Page/Page column 65 ;
WO 2010/002209 A2
