反应条件
1.1: lithium aluminium tetrahydride / diethyl ether / 5 h / 20 °C / |Inert atmosphere; |Cooling with ice 2.1: ethanol / |Inert atmosphere; |Reflux 3.1: sodium methylate / toluene / 0.33 h / |Inert atmosphere 3.2: 13 h / 60 °C / |Inert atmosphere 4.1: hydrogenchloride; zinc / ethanol; water / 20 °C / |Cooling with ice View Scheme
参考文献
Johansson, Henrik; Cailly, Thomas; Thomsen, Alex Rojas Bie; Braeuner-Osborne, Hans; Pedersen, Daniel Sejer
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1383 - 1387