反应条件
1.1: triethylamine / chloroform / 1 h / 20 °C
2.1: trichlorophosphate / 5 h / Reflux; Inert atmosphere
3.1: n-butyllithium / hexane / 2 h / -5 °C / Inert atmosphere
3.2: 2.75 h / -50 - 20 °C / Inert atmosphere
4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / 24 h / 110 °C / Inert atmosphere
View Scheme
参考文献
Xu, Qiu-Lei; Li, Hong-Yan; Wang, Cheng-Cheng; Zhang, Song; Li, Tian-Yi; Jing, Yi-Ming; Zheng, You-Xuan; Huang, Wei; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganica Chimica Acta, 2012 , vol. 391, p. 50 - 57