2,2,7,7-四甲基-3,5-辛二炔合成路线 （共 34 条）
反应条件
trimethylamine-N-oxide; sodium acetate; palladium dichloride; copper(l) iodide in acetonitrile T=20°C; 9 h;
参考文献
Li, Jin-Heng; Liang, Yun; Xie, Ye-Xiang
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4393 - 4396
反应条件
boron trifluoride diethyl etherate; difluoro[4-(trifluoromethyl)phenyl]-λ(3)-bromane in dichloromethane T=-78 - 20°C; 5 h;
参考文献
Ochiai, Masahito; Nishi, Yoshio; Goto, Satoru; Frohn, Hermann J.
Angewandte Chemie - International Edition, 2005 , vol. 44, # 3 p. 406 - 409
反应条件
tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide; trifuran-2-yl-phosphane in N,N-dimethyl-formamide T=80°C; homocoupling;
参考文献
Organic Letters, , vol. 2, # 18 p. 2857 - 2860
反应条件
bis(acetylacetonate)nickel(II); diisobutylaluminium hydride in diethyl ether; toluene T=-5°C; 1.5 h;
参考文献
Schwartz, Jeffrey; Carr, Denise B.; Hansen, Robert T.; Dayrit, Fabian M.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 3053 - 3061
反应条件
n-butyllithium; MNP dimer in tetrahydrofuran T=-60°C;
参考文献
Journal of the American Chemical Society, , vol. 110, p. 3272
反应条件
copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide T=80°C; 24 h; Inert atmosphere;
参考文献
Coste, Alexis; Couty, Francois; Evano, Gwilherm
Synthesis, 2010 , # 9 art. no. P16509SS, p. 1500 - 1504
反应条件
carbon monoxide; lithium chloride; tetracarbonylbis(μ-chloro)dirhodium(I) in tetrahydrofuran P=760 Torr; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 45, # 19 p. 3840 - 3846
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=80°C; 1 h;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 12 p. 2956 - 2966
反应条件
copper(l) iodide; triethylamine in N,N-dimethyl-formamide T=20°C; 16 h; Inert atmosphere;
参考文献
Li, Hongling; Wang, Lailai; Yang, Min; Qi, Yanxing
Catalysis Communications, 2012 , vol. 17, p. 179 - 183
反应条件
aluminium trichloride in dichloromethane T=-78°C; 2 h;
参考文献
Courtneidge, John L.; Davies, Alwyn G.; Gregory, Peter S.
Journal of the Chemical Society, Chemical Communications, 1986 , # 16 p. 1273 - 1275
