(E)-11-十六碳烯-1-醇合成路线 （共 15 条）
反应条件
pyridinium p-toluenesulfonate in methanol T=45°C; 3 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 11 p. 2296 - 2300
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2539 - 2544
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethylene glycol dimethyl ether T=140°C; 48 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, # 4.1 p. 621 - 624
Zhurnal Organicheskoi Khimii, , vol. 27, # 4 p. 722 - 727
反应条件
sodium hydroxide in ethanol 0.5 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 51, # 26 p. 5282 - 5286
反应条件
ammonia; lithium in tetrahydrofuran T=-60°C; 1 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 11 p. 2296 - 2300
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2539 - 2544
反应条件
1: 1.) ThxBHCl*Me2S, 2.) KIPBH, 3.) NaOMe, 4.) AcOH 2: 97 percent / 20percent aq. NaOH / aq. ethanol / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 26 p. 5282 - 5286
反应条件
1: 1.) ThxBHCl*Me2S, 2.) KIPBH, 3.) NaOMe, 4.) AcOH 2: 97 percent / 20percent aq. NaOH / aq. ethanol / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 26 p. 5282 - 5286
反应条件
1: 1) Mg, 2) Li2CuCl4 / 1) THF, 2) THF, a) -70 deg C to 20 deg C over 45 min, b) 2 h at 20 deg C 2: 92 percent / TsOH*Py / methanol / 3 h / 45 °C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 11 p. 2296 - 2300
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2539 - 2544
反应条件
1: 1.) lithium amide / 1.) HMPTA, RT, 1.5 h, 2.) HMPTA, 25 deg C, 8 h 2: 56.3 percent / LiAlH4 / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 48 h / 140 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, # 4.1 p. 621 - 624
Zhurnal Organicheskoi Khimii, , vol. 27, # 4 p. 722 - 727
反应条件
1: 1.) lithium amide / 1.) HMPTA, RT, 1.5 h, 2.) HMPTA, 25 deg C, 8 h 2: 56.3 percent / LiAlH4 / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 48 h / 140 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, # 4.1 p. 621 - 624
Zhurnal Organicheskoi Khimii, , vol. 27, # 4 p. 722 - 727
反应条件
1: 90 percent / acetonitrile 2: DMSO, NaH / tetrahydrofuran / 0.5 h View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 44, # 2 p. 257 - 261
