2,2-二氯乙酰乙酸乙酯合成路线 （共 16 条）
反应条件
chlorine
T=55 - 60°C; 9 h; dinamics of chlorination of acetoacetic ester, products in the mixture on the time; Product distributionMechanism;
参考文献
Amriev; Velichko; Abdulkina
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 111 pt 1 p. 2318 - 2322
参考文献
Macbeth
Journal of the Chemical Society, 1923 , vol. 123, p. 1129
参考文献
Castro,B. et al.
Bulletin de la Societe Chimique de France, 1969 , p. 3521 - 3522
反应条件
nitryl chloride in dichloromethane
T=20°C; 2 h; variation of molar ratio of NO2Cl/educt, solvent, temperature and add. of CaCl2 or Na2SO4; Product distribution;
参考文献
Prostenik, Mladen V.; Dumic, Miljenko; Bosnjak, Nada
Monatshefte fuer Chemie, 1980 , vol. 111, p. 771 - 774
反应条件
(i) iPrMgCl, THF, (ii) /BRN= 385737/; Multistep reaction;
参考文献
Villieras,B.; Castro,B.
Bulletin de la Societe Chimique de France, 1968 , p. 246 - 250
反应条件
pentacarbonyliron(0); N,N-dimethyl-formamide
T=140°C; 2 h; other reagents, temperature, reagents ratios; Product distribution;
参考文献
Abdulkina, Z. A.; Amriev, R. A.; Velichko, F. K.; Mysov, E. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 4 p. 605 - 608
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 4 p. 824 - 827
