7-苯基-2,5-庚烷二酮合成路线 （共 18 条）
反应条件
samarium diiodide in tetrahydrofuran; methanol; N,N,N',N',N'',N''-hexamethylphosphoric triamide Heating;
参考文献
Bradley; Williams; Blann, Kevin; Caddy, Judy
Organic Preparations and Procedures International, 2001 , vol. 33, # 6 p. 565 - 602
反应条件
5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride; triethylamine in ethanol
T=80°C; Stetter coupling;
参考文献
Cranwell, Philippa B.; O'Brien, Matthew; Browne, Duncan L.; Koos, Peter; Polyzos, Anastasios; Pena-Lopez, Miguel; Ley, Steven V.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 30 p. 5774 - 5779
反应条件
triethylamine in ethanol
参考文献
Bayer Aktiengesellschaft
Patent: US4035395 A1, 1977 ;
反应条件
[RuCl2(dppm)(NCCH3)2]; water in 1,4-dioxane
T=100°C; 24 h;
参考文献
Chen, Yiyun; Park, Sung Hwan; Lee, Chung Whan; Lee, Chulbom
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2000 - 2004
反应条件
1: diiodomethane With diethylzinc; trifluoroacetic acid in dichloromethane
T=0°C; 0.5 h;
2: 6-phenyl-hexane-2,4-dione in dichloromethane
T=20°C; 5 h;
参考文献
Xue, Song; Li, Le-Zhen; Liu, Yong-Kang; Guo, Qing-Xiang
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 215 - 218
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
Heating;
参考文献
Perez, Marta; Castano, Ana M.; Echavarren, Antonio M.
Journal of Organic Chemistry, 1992 , vol. 57, # 19 p. 5047 - 5049
反应条件
benzoic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene
T=110°C; 24 h; Title compound not separated from byproducts.;
参考文献
Pridmore, Simon J.; Slatford, Paul A.; Williams, Jonathan M.J.
Tetrahedron Letters, 2007 , vol. 48, # 29 p. 5111 - 5114
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Nimgirawath,S. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 339 - 356
反应条件
1: aq. NaOH / ethanol
2: H2 / Pd-C / ethanol
View Scheme
参考文献
Nimgirawath,S. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 339 - 356
反应条件
1: aq. H2SO4 / ethanol
2: aq. NaOH / ethanol
3: H2 / Pd-C / ethanol
View Scheme
参考文献
Nimgirawath,S. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 339 - 356
