Camilleri, Patrick; Clark, Michael T.; Gilmore, Ian J.; Cole-Hamilton, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 833 - 836
1: 60percent NaH / toluene; tetrahydrofuran / Ambient temperature
2: NH2OH*HCl; NaOAc*H2O / ethanol; H2O / 0.5 h
3: 46 percent / SCl2; iodine / tetrahydrofuran / -70 - -40 °C
View Scheme
参考文献
Camilleri, Patrick; Clark, Michael T.; Gilmore, Ian J.; Cole-Hamilton, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 833 - 836
1: 60percent NaH / toluene; tetrahydrofuran / Ambient temperature
2: NH2OH*HCl; NaOAc*H2O / ethanol; H2O / 0.5 h
3: 46 percent / SCl2; iodine / tetrahydrofuran / -70 - -40 °C
4: 70 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.25 h / Ambient temperature
View Scheme
参考文献
Camilleri, Patrick; Clark, Michael T.; Gilmore, Ian J.; Cole-Hamilton, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 833 - 836
1: 60percent NaH / toluene; tetrahydrofuran / Ambient temperature
2: NH2OH*HCl; NaOAc*H2O / ethanol; H2O / 0.5 h
3: 46 percent / SCl2; iodine / tetrahydrofuran / -70 - -40 °C
4: 64 percent / m-chloroperbenzoic acid / CHCl3 / 2 h / 40 °C
View Scheme
参考文献
Camilleri, Patrick; Clark, Michael T.; Gilmore, Ian J.; Cole-Hamilton, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 833 - 836