2-(2-呋喃基)-2-己醇合成路线 (共 2 条)
反应条件
1: 1-bromo-butane With magnesium; ethylene dibromide in 2-methyl tetrahydrofuran
T=20°C; Inert atmosphere;
2: 2-acetyl-furan in 2-methyl tetrahydrofuran
T=0 - 20°C; Grignard reaction; 1.75 h; Inert atmosphere; chemoselective reaction;
参考文献
Zhong, Weihui; Wu, Yaotiao; Zhang, Xingxian
Journal of Chemical Research, 2009 , # 6 p. 370 - 373
反应条件
in diethyl ether
Heating;
参考文献
Fischer, Petra; Segovia, Ana Belen Garcia; Gruner, Margit; Metz, Peter
Angewandte Chemie - International Edition, 2005 , vol. 44, # 38 p. 6231 - 6234