4-氯-1,1-二乙氧基丁烷合成路线 （共 12 条）
反应条件
amberlyst-15; orthoformic acid triethyl ester in water Heating;
参考文献
Hyatt, John Anthony
Patent: US2004/192958 A1, 2004 ;
Location in patent: Page 3-4 ;
反应条件
sodium hydroxide; CaCl2; hydrogen; hydrogen sulfide in quinoline; ethanol; water; toluene
参考文献
Journal of the American Chemical Society, , vol. 73, p. 1365
参考文献
Australian Journal of Scientific Research, Series A: Physical Sciences, , vol. 3, p. 336,339
反应条件
(i) Pd-BaSO4, quinoline, sulfur, xylene, (ii) /BRN= 605384/; Multistep reaction;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 88, p. 177 - 184
反应条件
potassium iodide in dimethyl sulfoxide T=100°C; 20 h;
参考文献
Veerman, Johan J. N.; Klein, Jasper; Aben, Rene W. M.; Scheeren, Hans W.; Kruse, Chris G.; Van Maarseveen, Jan H.; Rutjes, Floris P. J. T.; Hiemstra, Henk
European Journal of Organic Chemistry, 2002 , # 18 p. 3133 - 3139
反应条件
ethylene glycol; potassium iodide T=100°C;
参考文献
Anet et al.
Australian Journal of Scientific Research, Series A: Physical Sciences, 1950 , vol. 3, p. 336,339
反应条件
1: 71 percent / KI / dimethylsulfoxide / 20 h / 100 °C 2: 55 percent / LiAlH4 / diethyl ether / 3 h / 0 °C View Scheme
参考文献
Anet et al.
Australian Journal of Scientific Research, Series A: Physical Sciences, 1950 , vol. 3, p. 336,339
反应条件
1: in methanol 48 h; 2: With sodium hydroxide in water
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 48, # 4 p. 590 - 594
反应条件
(i) liq. NH3, (ii) NaNH2; Multistep reaction;
参考文献
Ward,J.P.; van Dorp,D.A.
Recueil des Travaux Chimiques des Pays-Bas, 1969 , vol. 88, p. 177 - 184
