反应条件
1: 1.) Na 2.) H2 / 2.) 10percent Pd/C / 1.) EtOH, 2.) EtOH, RT, atm. pressure, 6 h 2: 3.2 g / K2CO3 / acetone / 24 h / Ambient temperature 3: 1.4 g / SOCl2, HCl / CHCl3 / 1.5 h / Heating 4: ethanol / 30 h / 100 °C 5: 0.7 g / H2 / 10percent Pd/C / ethanol / 5 h / 50 °C View Scheme
参考文献
Balsamo, A.; Giorgi, I.; Lapucci, A.; Lucacchini, A.; Macchia, B.; et al.
Journal of Medicinal Chemistry, 1987 , vol. 30, # 1 p. 222 - 225
