反应条件
sealed evacuated ampoule, Sb-compd. heating (220°C for 1 h), cooling, ethyl bromide addn., bromination; solvent removing, residue extracting with petroleum ether and passing through column with alumina, eluate evapn. (yielding ester), residue re-crystn. (benzene-isopropanol) yielding Sb-compd.;
参考文献
Russian Journal of General Chemistry, , vol. 67, # 9 p. 1443 - 1448