反应条件
(n)BuLi in tetrahydrofuran BuLi addn. to TosMIC soln. (198-208 K), M33SnCl dropwise addn., PhCHCHCOPh addn., stirring (2 h, temp. rise to 233 K), quenching with water; ether extraction, washing (water), drying, evapn., crystn. (CH2Cl2/hexane);
参考文献
Meetsma; Dijkstra; Have; Van Leusen
Acta Crystallographica, Section C: Crystal Structure Communications, 1996 , vol. 52, # pt 11 p. 2747 - 2750