2'-溴-4'-甲基乙酰苯胺合成路线 （共 38 条）
反应条件
palladium diacetate; potassium carbonate; [(t-Bu)3PH]BF4 in toluene T=140°C; Microwave irradiationSealed vessel;
参考文献
Myers, Jeffery T.; Hanna Jr., James M.
Tetrahedron Letters, 2012 , vol. 53, # 6 p. 612 - 615
反应条件
potassium carbonate; butan-1-ol; palladium diacetate; triphenylphosphine T=100°C; 14 h;
参考文献
Chen, Jingbo; Zhang, Yushun; Yang, Liquan; Zhang, Xiang; Liu, Jianping; Li, Liang; Zhang, Hongbin
Tetrahedron, 2007 , vol. 63, # 20 p. 4266 - 4270
反应条件
nitric acid Destillieren des entstandenen Acetylderivates mit Natronlauge;
参考文献
Cohen; Dutt
Journal of the Chemical Society, 1914 , vol. 105, p. 514
反应条件
1: nitric acid / Destillieren des entstandenen Acetylderivates mit Natronlauge 2: bei der Entamidierung View Scheme
参考文献
Wroblewski
Justus Liebigs Annalen der Chemie, 1878 , vol. 192, p. 203
参考文献
Nicolet
Journal of the American Chemical Society, 1921 , vol. 43, p. 2083
参考文献
Nicolet
Journal of the American Chemical Society, 1921 , vol. 43, p. 2083
反应条件
hydrogenchloride in ethanol 4 h; Heating; Yield given;
参考文献
Chaudhuri, Narayan C.
Synthetic Communications, 1996 , vol. 26, # 20 p. 3783 - 3790
反应条件
1: 99 percent / Pd(OAc)2; 2-dicyclohexylphosphino-2',6'-dimethoxy-1,1'-biphenyl; K3PO4 / toluene / 0.25 h / 90 °C 2: 92 percent / Pd(OAc)2; molecular sieves 3 Angstroem; Cu(OAc)2 / O2 / toluene / 120 °C View Scheme
参考文献
Tsang, W. C. Peter; Zheng, Nan; Buchwald, Stephen L.
Journal of the American Chemical Society, 2005 , vol. 127, # 42 p. 14560 - 14561
反应条件
1: conc.HCl / aq. ethanol / 4 h / Heating 2: NaOH / H2O / 0.5 h / Ambient temperature 3: 75 percent / dimethylformamide / 4 h / 160 °C View Scheme
参考文献
Chaudhuri, Narayan C.
Synthetic Communications, 1996 , vol. 26, # 20 p. 3783 - 3790
参考文献
Nicolet
Journal of the American Chemical Society, 1921 , vol. 43, p. 2083
