5-甲基-5H-吡啶并[4,3-b]吲哚合成路线 （共 5 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=160°C; 7 h;
参考文献
Sako, Kumiko; Aoyama, Hiroshi; Sato, Shinichi; Hashimoto, Yuichi; Baba, Masanori
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 7 p. 3780 - 3790
反应条件
1: 94 percent / Et3N; 1percent CuI / 2percent PdCl2(PPh3)2 / dimethylformamide / 16 h / 60 °C
2: 41 percent / tert-butylamine / 94 h / 100 - 130 °C
View Scheme
参考文献
Zhang, Haiming; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 20 p. 7048 - 7056
反应条件
tert-butylamine
T=100 - 130°C; 94 h;
参考文献
Zhang, Haiming; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 20 p. 7048 - 7056
反应条件
1: 100 percent / 22 h / 100 °C
2: 40 percent / 10percent CuI / dimethylformamide / 94 h / 100 - 130 °C
View Scheme
参考文献
Zhang, Haiming; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 20 p. 7048 - 7056
反应条件
sodium; 1-methyl-naphthalene
Erwaermen des Reaktionsgemisches mit CH3I und anschliessenden Erhitzen unter vermindertem Druck;
参考文献
Eiter
Monatshefte fuer Chemie, 1948 , vol. 79, p. 17,20
