3-甲基-2-呋喃甲酸甲酯合成路线 （共 16 条）
参考文献
Knight, David W.; Rustidge, David C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 679 - 683
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 15 h; Heating / reflux;
参考文献
BAYER CROPSCIENCE AKTIENGESELLSCHAFT
Patent: WO2003/99009 A1, 2003 ;
Location in patent: Page 42, 43 ;
反应条件
sodium hydroxide in ethanol; water
参考文献
Uniroyal Chemical Company, Inc.; Uniroyal Chemical Ltd./Ltee
Patent: US5268389 A1, 1993 ;
反应条件
1: aq. NaOH solution 2: copper; quinoline View Scheme
参考文献
Montana, Angel M.; Castellvi, Maria; Batalla, Consuelo; Grima, Pedro M.; Font-Bardia, Merce
Tetrahedron, 2012 , vol. 68, # 48 p. 9982 - 9998,17
Title/Abstract Full Text Show Details
Montana, Angel M.; Grima, Pedro M.; Castellvi, Maria; Batalla, Consuelo; Font-Bardia, Merce
Tetrahedron, 2012 , vol. 68, # 48 p. 9982 - 9998
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether
T=20°C;
参考文献
Baldwin, Jack E.; Mayweg, Alexander V.W.; Pritchard, Gareth J.; Adlington, Robert M.
Tetrahedron Letters, 2003 , vol. 44, # 24 p. 4543 - 4545
反应条件
1: 63 percent / NaOMe, HCONH2 / 0.5 h / 100 °C
2: LiAlH4 / tetrahydrofuran / 5 h / 50 - 60 °C
View Scheme
参考文献
Katsura, Yousuke; Nishino, Shigetaka; Ohno, Mitsuko; Sakane, Kazuo; Matsumoto, Yoshimi; Morinaga, Chizu; Ishikawa, Hirohumi; Takasugi, Hisashi
Journal of Medicinal Chemistry, 1999 , vol. 42, # 15 p. 2920 - 2926
