N,n,4-三甲基噻唑-2-胺合成路线 （共 10 条）
反应条件
piperidine in ethanol
1.) 20 deg C, 2.) reflux, 3 h;
参考文献
Brown, Michael D.; Gillon, David W.; Meakins, G. Denis; Whitham, Gordon H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1623 - 1626
反应条件
triethylamine in ethanol
1.) 20 deg C, 30 min, 2.) reflux, 3 h;
参考文献
Brown, Michael D.; Gillon, David W.; Meakins, G. Denis; Whitham, Gordon H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1623 - 1626
反应条件
sodium hydrogensulfide; triethylamine in ethanol
1.) 20 deg C, 2.) reflux;
参考文献
Brown, Michael D.; Gillon, David W.; Meakins, G. Denis; Whitham, Gordon H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1623 - 1626
反应条件
boron trifluoride diethyl etherate in diethyl ether
8 h; Ambient temperature;
参考文献
Jong, R.L.P. de; Meijer, J.; Sukhai, R.S.; Bradsma, L.
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 9 p. 310 - 313
反应条件
in ethanol
2 h; Heating;
参考文献
Gillon, David W.; Forrest, Ian J.; Meakins, G. Denis; Tirel, Malcolm D.; Wallis, John D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 341 - 348
参考文献
Mahon, Catherine M.; Meakins, G.D.
Journal of Chemical Research, Miniprint, 1990 , # 9 p. 2083 - 2090
参考文献
Ohtsuka; Toyofuku; Miyasaka; Arakawa
Chemical and Pharmaceutical Bulletin, 1975 , vol. 23, # 12 p. 3234 - 3242
参考文献
Garreau
Bulletin de la Societe Chimique de France, 1954 , p. 1048,1052
反应条件
trichlorophosphate
T=40°C; 4 h;
参考文献
Gillon, David W.; Forrest, Ian J.; Meakins, G. Denis; Tirel, Malcolm D.; Wallis, John D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 341 - 348
反应条件
sulfuric acid; nitric acid
T=20°C; Yield given;
参考文献
Birkinshaw, Timothy N.; Gillon, David W.; Harkin, Shaun A.; Meakins, G. Denis; Tirel, Malkom D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 147 - 153
