1-(4,6-二羟基-3-((2-羟基苯基)甲基)-2-甲氧基苯基)-3-苯基-1-丙酮合成路线 （共 10 条）
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
P=760 Torr; Ambient temperature;
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 0.55 g / BF3*Et2O / dioxane / 3 h / 60 - 70 °C
2: 0.18 g / K2CO3, KI / acetone / 9 h / Heating
3: 0.23 g / aq. KOH / dimethylsulfoxide; ethanol / Ambient temperature
4: 15 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 0.55 g / BF3*Et2O / dioxane / 3 h / 60 - 70 °C
2: 0.18 g / K2CO3, KI / acetone / 9 h / Heating
3: 0.23 g / aq. KOH / dimethylsulfoxide; ethanol / Ambient temperature
4: 15 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 12.0 g / K2CO3 / dimethylformamide / 7 h / Heating
2: 10.0 g / KOH, 40percent formalin / methanol / 3 h / 60 - 70 °C
3: 0.55 g / BF3*Et2O / dioxane / 3 h / 60 - 70 °C
4: 0.18 g / K2CO3, KI / acetone / 9 h / Heating
5: 0.23 g / aq. KOH / dimethylsulfoxide; ethanol / Ambient temperature
6: 15 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 10.0 g / KOH, 40percent formalin / methanol / 3 h / 60 - 70 °C
2: 0.55 g / BF3*Et2O / dioxane / 3 h / 60 - 70 °C
3: 0.18 g / K2CO3, KI / acetone / 9 h / Heating
4: 0.23 g / aq. KOH / dimethylsulfoxide; ethanol / Ambient temperature
5: 15 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 0.36 g / KOH / methanol / 24 h / Ambient temperature
2: 0.18 g / K2CO3, KI / acetone / 9 h / Heating
3: 0.23 g / aq. KOH / dimethylsulfoxide; ethanol / Ambient temperature
4: 15 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 0.23 g / aq. KOH / dimethylsulfoxide; ethanol / Ambient temperature
2: 15 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 0.18 g / K2CO3, KI / acetone / 9 h / Heating
2: 0.23 g / aq. KOH / dimethylsulfoxide; ethanol / Ambient temperature
3: 15 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 0.23 g / aq. KOH / dimethylsulfoxide; ethanol / Ambient temperature
2: 15 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
参考文献
Lasswell,W.L.; Hufford,C.D.
Journal of Organic Chemistry, 1977 , vol. 42, # 8 p. 1295 - 1302
