(R)-1,2-十六烷二醇合成路线 (共 6 条)
反应条件
AD-mix-β in water; tert-butyl alcohol
T=4°C; 40 h; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Li, Shengrong; Pang, Jihai; Wilson, William K.; Schroepfer Jr., George J.
Tetrahedron Asymmetry, 1999 , vol. 10, # 9 p. 1697 - 1707
反应条件
AD-mix-β in water; tert-butyl alcohol
T=0°C; dihydroxylation;
参考文献
He, Linli; Byun, Hoe-Sup; Bittman, Robert
Journal of Organic Chemistry, 2000 , vol. 65, # 22 p. 7618 - 7626
反应条件
Jacobsen's (S,S)-(salen)Co(III) catalyst; water in tetrahydrofuran
T=0°C; 6 h;
参考文献
Lafont, Dominique; Bouchu, Marie-Noelle; Girard-Egrot, Agnes; Boullanger, Paul
Carbohydrate Research, 2001 , vol. 336, # 3 p. 181 - 194
参考文献
Lafont, Dominique; Bouchu, Marie-Noelle; Girard-Egrot, Agnes; Boullanger, Paul
Carbohydrate Research, 2001 , vol. 336, # 3 p. 181 - 194
反应条件
1: 48 percent / (R,R)-(-)-(Salen)Co(III); H2O / tetrahydrofuran / 6 h / 0 °C
2: 78 percent / H2O
View Scheme
参考文献
Lafont, Dominique; Bouchu, Marie-Noelle; Girard-Egrot, Agnes; Boullanger, Paul
Carbohydrate Research, 2001 , vol. 336, # 3 p. 181 - 194
反应条件
lithium aluminium tetrahydride
参考文献
Horn; Hougen
Journal of the Chemical Society, 1953 , p. 3533,3537