1: With hydrogenchloride; thionyl chloride in N,N-dimethyl-formamide
T=5°C; 3 h; Inert atmosphere;
2: With hydrogenchloride in diethyl ether
T=0°C; Inert atmosphere;
参考文献
Yan, Ni; Xu, Zhiyan; Diehn, Kevin K.; Raghavan, Srinivasa R.; Fang, Yu; Weiss, Richard G.
Journal of the American Chemical Society, 2013 , vol. 135, # 24 p. 8989 - 8999
1: With sodium hydroxide in dichloromethane
2: With hydrogenchloride; thionyl chloride in diethyl ether; dichloromethane; N,N-dimethyl-formamide
T=0°C;
Yan, Ni; Xu, Zhiyan; Diehn, Kevin K.; Raghavan, Srinivasa R.; Fang, Yu; Weiss, Richard G.
Journal of the American Chemical Society, 2013 , vol. 135, # 24 p. 8989 - 8999