反应条件
1: 1) conc. HCl, NaNO2, 2) 1M KOH / 1) water, 10 min, ice bath, 2) 30 min, ice bath 2: 1) sec-BuLi / 1) ether, hexane, 30 min, -78 deg C, 2) -78 deg C to r.t. 3: 37 percent / 1M KOH, Al-Ni alloy / methanol / 18 h / Ambient temperature View Scheme
参考文献
Gross, Margaret L.; Blank, David H.; Welch, Willard M.
Journal of Organic Chemistry, 1993 , vol. 58, # 8 p. 2104 - 2109