1: With 2 mol Pd/C; sodium carbonate in N,N-dimethyl-formamide T=120°C; Larock heteroannulation; 18 h; Inert atmosphere; 2: With hydrogenchloride in water regioselective reaction;
Stokes, Benjamin J.; Jovanovic, Brankica; Dong, Huijun; Richert, Kathleen J.; Riell, Ryan D.; Driver, Tom G.
Journal of Organic Chemistry, 2009 , vol. 74, # 8 p. 3225 - 3228
1: 76 percent / benzoquinone, lithium chloride / dichlorobis(acetonitrile)palladium(II) / tetrahydrofuran / 24 h / Ambient temperature 2: 95 percent / triethylamine / palladium(II) acetate, tri-o-tolylphosphine / acetonitrile / 20 h / 100 °C View Scheme
参考文献
Kasahara, Akira; Izumi, Taeko; Murakami, Satoshi; Yanai, Hiroshi; Takatori, Masayuki
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 3 p. 927 - 928
