1: 24 h / 70 °C 2: 1,5,7-triazabicyclo[4.4.0]dec-5-ene bound to polystyrene / acetonitrile / 5 h / 20 °C 3: tris-(dibenzylideneacetone)dipalladium(0); triethylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 12 h / 110 °C View Scheme
(+/-)-BINAP; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate in toluene Buchwald-Hartwig reaction; Reflux;
参考文献
Buckley, Benjamin R.; Christie, Steven D. R.; Elsegood, Mark R. J.; Gillings, Claire M.; Page, Philip C. Bulman; Pardoe, William J. M.
Synlett, 2010 , # 6 p. 939 - 943
