sulfuric acid T=25°C; further reagent; Product distribution;
参考文献
Cerfontain, Hans; Koeberg-Telder, Ankie; Laali, Khosrow; Lambrechts, Hans J. A.; Wit, Peter de
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 11 p. 390 - 392
1: With lithium amide; [(CyPF-tBu)PdCl2] in ethylene glycol dimethyl ether T=80°C; 24 h; Sealed vial; 2: With hydrogenchloride in ethylene glycol dimethyl ether; water T=20°C; 0.0833333 h; 3: With sodium hydrogencarbonate in ethylene glycol dimethyl ether; water Product distribution / selectivity;
参考文献
YALE UNIVERSITY
Patent: WO2007/109365 A2, 2007 ;
Location in patent: Page/Page column 48-49; 51 ;
in dimethyl sulfoxide Kinetics; byproducts: o-MeC6H4NPh2, p-MeC6H4NPh2; heating of ((phen)2Cu)(Cu(NPh2)2) with mixt. of o- and p-iodotoluene (20equiv. of each) in DMSO at 80°C for 3 h or at 30°C with a dded CuI;
参考文献
Giri, Ramesh; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 15860 - 15863
in dimethyl sulfoxide byproducts: o-MeC6H4NPh2, p-MeC6H4NPh2; heating of K(Cu(NPh2)2) with mixt. of o- and p-iodotoluene (20 equiv. ofeach) in DMSO at 80°C for 3 h with added CuI;
参考文献
Giri, Ramesh; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 15860 - 15863
in dimethyl sulfoxide byproducts: o-MeC6H4NPh2, p-MeC6H4NPh2; heating of (K(18-crown-6))(Cu(NPh2)2) with mixt. of o- and p-iodotoluene(20 equiv. of each) in DMSO at 80°C for 3 h with added CuI (1 eq uiv.);
参考文献
Giri, Ramesh; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 15860 - 15863
in dimethyl sulfoxide Kinetics; byproducts: o-MeC6H4NPh2, p-MeC6H4NPh2; heating of (Li(phen)3)(Cu(NPh2)2) with mixt. of o- and p-iodotoluene (20equuv. of each) in DMSO at 100°C for 3 h or at 80°C with added 4 equiv. of CuI;
参考文献
Giri, Ramesh; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 15860 - 15863
